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标题:Reactions of organozinc reagents with potassium bromodifluoroacetate
时间:2021-07-30 14:42:42
DOI:10.1016/j.jfluchem.2014.08.021
大小:789 kb
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目录:
  • Reactions of organozinc reagents with potassium bromodifluoroacetate
    • 1 Introduction
    • 2 Results and discussion
    • 3 Conclusions
    • 4 Experimental
      • 4.1 General experimental procedures
      • 4.2 3-Bromobutyl benzoate
      • 4.3 Synthesis of products 4 and 5a
        • 4.3.1 (2,2-Difluoroethyl)benzene (4) [18]
        • 4.3.2 (2-Bromo-2,2-difluoroethyl)benzene (5a)
      • 4.4 Preparation of 5b–i (general procedure)
        • 4.4.1 1-Bromo-4-(2-bromo-2,2-difluoroethyl)benzene (5b)
        • 4.4.2 1-Bromo-2-(2,2-difluoropent-4-en-1-yl)benzene (5c)
        • 4.4.3 2-(2-Bromo-2,2-difluoroethyl)phenyl benzoate (5d)
        • 4.4.4 1-(2-Bromo-2,2-difluoroethyl)naphthalene (5e)
        • 4.4.5 Diethyl (3-bromo-3,3-difluoropropyl)phosphonate (5f)
        • 4.4.6 Ethyl 5,5-difluoro-7-methyloct-7-enoate (5g)
        • 4.4.7 4,4-Difluorobutyl benzoate (5h)
        • 4.4.8 4-Bromo-4,4-difluoro-3-methylbutyl benzoate (5i)
    • Acknowledgment
    • References

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