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标题:Enhanced electrocatalytic dechlorination of para -chloronitrobenzene based on Ni/Pd foam electrode
时间:2020-01-14 23:01:08
DOI:10.1016/j.cej.2017.01.024
大小:1024 kb
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目录:
  • Enhanced electrocatalytic dechlorination of para-chloronitrobenzene based on Ni/Pd foam electrode
    • 1 Introduction
    • 2 Materials and methods
      • 2.1 Chemicals and electrodes
      • 2.2 Preparation of cathode
      • 2.3 Characterization
      • 2.4 Electrochemical experiments
      • 2.5 Analytical methods
    • 3 Results and discussion
      • 3.1 Characterization and performance of Ni/Pd foam electrodes
        • 3.1.1 Physical characterizations
        • 3.1.2 Cyclic voltammetry and degradation kinetics
        • 3.1.3 Electrocatalytic reduction of p-CNB with different cathodes
        • 3.1.4 Appropriate content of Pd on Ni/Pd foam electrodes
      • 3.2 Major factors influencing dechlorination of p-CNB
        • 3.2.1 Effect of current density on p-CNB reduction
      • 3.3 Effect of initial pH on p-CNB reduction
        • 3.3.1 Effect of electrolyte concentration on p-CNB reduction
      • 3.4 Electrochemical reduction pathway of p-CNB
    • 4 Conclusion
    • Acknowledgments
    • Appendix A Supplementary data
    • References

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