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标题:Analysis of thermally labile pesticides by on-column injection gas chromatography in fruit and vegetables.
时间:2019-06-12 23:32:23
DOI:10.1007/s00216-018-1286-1
PMID:30105623
作者:Samanta Uclés;Elena Hakme;Carmen Ferrer;Amadeo R. Fernández-Alba
出版源: Analytical and Bioanalytical Chemistry ,2018
摘要:Analysis of thermally labile pesticides by on-column injection gas chromatography in fruit and vegetablesThermally labile pesticides (captafol, captan, dicofol, and folpet) are highly prone to suffer thermal degradation during sample introduction into a gas chromatograph (GC) to tetrahydrophthalimide...doi:10.1007/s00216-018-1286-1Samanta Uclés...
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目录:
  • Analysis of thermally labile pesticides by on-column injection gas chromatography in fruit and vegetables
    • Abstract
    • Introduction
    • Materials and methods
      • Reagents and materials
      • GC-MS/MS instruments
      • Sample preparation
      • Degradation study
      • Method validation
    • Results and discussion
      • Degradation study
      • Linearity
      • Matrix effect
      • Recoveries and repeatability
      • Limit of quantitation
      • Application to a proficiency test
    • Conclusions
    • References

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